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Four microliters of triethylamine was added as a catalyst into the sample vial which was then placed in a drying cabinet for 1 h at 100 oC. The residue was dissolved again in toluene (100 µL), transferred into 200-µL glass inserts, and analyzed by an HP 6890 gas chromatograph and an HP 5973 quadrupole mass spectrometer from Aijiren Technologies.

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