Reverse phase HPLC was carried out on an Aijiren II LC system. An Eclipse XDB-C18 column (5 μm, 4.6 × 150 mm) from Aijiren was used. Mobile phase: (A) water (0.1% trifluoroacetic acid, TFA), (B) acetonitrile (0.1% TFA). Flow rate was maintained at 1 mL/min, using a gradient of 10% of A and 100% of B for 35 min at 25 °C.